Composites Design and Manufacture (BEng) - MATS 324
Non-Destructive Testing (NDT) of advanced composites. |
PowerPoint presentation (778 KB file)
NetComposites NDT Selection Tool
Summerscales [1-3] and Burt and Smith [4] have reviewed the use of non-destructive evaluation/examination (NDE) or NDT for fibre-reinforced
composite materials. The applications of NDE/NDT can be considered to fulfil three functions:
| For samples in the laboratory |
For structures during manufacture and service |
|
initial inspection of test
samples |
confirmation of structural
integrity |
|
monitoring sample tests in
progress |
monitoring components under
service loads, especially when changing over time |
|
analysis of reasons for failure
|
analysis of reasons for failure
|
The various techniques can be arranged under three categories and further sub-divided
by
operating frequency albeit that some overlap may occur:
In the list which follows, references are provided for recent books or review articles pertinent to each topic
(referencing under development). Working from high frequency/short wavelength, the various techniques in each of the three categories are:
- The electromagnetic spectrum.
- radiography
- x-ray computed microtomography (X-ray μCT) [5-7]
- ultraviolet
- visible light
- liquid penetrants and brittle lacquers
- edge replication and the de-ply technique
- optical fringes
- photoelasticity
- optical caustics
- coherent light
- interferometry [8]
- holography
- speckle [9]
- shearography
- embedded optical fibres
- Fibre Bragg Gratings (FBG) are regular
periodic changes in the refractive index of the core of an optical fibre
over a short distance. The grating acts as an in-line optical
filter (reflector) at a specific wavelength governed by the grating
spacing. Under strain, the spacing changes in a linear manner
which can be monitored as a peak in the reflected signal or a trough in
the transmitted signal.
- Chirped Fibre Bragg Gratings (CFBG) may be up to 120 mm in length
and have a linear increase in the grating spacing. The reflection
peak/transmission trough becomes a plateau corresponding to the length
of the FBG. Under uniform strain, the whole plateau moves, while
perturbation on the plateau can indicate the position of damage.
- near-infrared [10]
- thermography [11, 12]
- externally applied thermal field (EATF)
- stress generated thermal field (SGTF), including
- vibrothermography (low frequency mechanical excitation), and
- thermosonics (ultrasonic excitation)
- terahertz spectroscopy [13-16]
- Thz technology is a relatively new field facilitated by the development of femtosecond pulsed lasers
and the semiconductor
Quantum Cascade Laser (QCL). A "most pressing component technology development remains in
the area of terahertz sources [with significant power output]"
[Siegel, 13] which
may be addressed by the use of "designer spoof surface
plasmon structures" to collimate terahertz laser beams
[17]. The technology is already attracting significant interest in the context of security
applications.
- microwaves
- eddy current
- dielectric [18, 19]
- electric
- Spectroscopy.
- ultraviolet
- Raman [20]
- infrared
- electron spin resonance
- nuclear magnetic resonance
- Kotsikos et al [21] have used nuclear magnetic resonance imaging to study seawater uptake in marine fibreglass composites.
- Mechanical vibration.
- scanning acoustic microscopy
- ultrasonics [22]
- ultrasound data can be presented in a number of ways:
- A-scan: voltage/time at one position (see Flash Movie animation by Wavelength-NDT)
- B-scan: size and position vs probe movement (see Flash Movie animation by Wavelength-NDT)
- C-scan: attenuation vs x-y position (see Flash Movie animation by Wavelength-NDT)
- D-scan: attenuation vs x-z position
- F-scan: feature scan
- P-scan: projection/tomography
- S-scan: sector scan (phased array technique)
- phased arrays [23]: transducers containing an array of elements
which are individually wired, individually pulsed and where each can be
time-shifted relative to other elements of the array by delays accurate
to ~2 nanoseconds.
- Smith et al [24] have recently presented the state-of-the-art in
automated analysis and advanced defect detection from ultrasonic
scans of composites.
- acousto-ultrasonics
- acoustic emission
- Kaiser effect
- Felicity effect
- CARP (Committee on Acoustic Emission from Reinforced Plastics) procedures, for example:
- ASTM E976-05 (2005) Standard guide for determining the reproducibility of acoustic emission sensor response
- ASTM E1067-01 (2001) Standard practice for acoustic emission examination of fibreglass reinforced plastic resin (FRP) tanks/vessels.
- ASTM E1118-05 (2005) Standard practice for acoustic emission examination of reinforced thermosetting resin pipe (RTRP).
- ASTM E2076-05 (2005) Standard test method for examination of fiberglass reinforced plastic fan blades using acoustic emission.
- ASTM E2191-02 (2002) Standard test method for examination of gas-filled filament-wound composite pressure vessels using acoustic emission.
- ASTM E2478-06 (2006) Standard practice for determining damage-based design criteria for fiberglass reinforced plastics (FRP) materials.
- ASTM F914-03 (2003) Standard test method for acoustic emission for insulated and non-insulated aerial personnel devices without supplemental load handling attachments.
- ASTM F1430-03e1 (2003) Standard test method for acoustic emission testing of insulated and non-insulated aerial personnel devices with supplemental load handling attachments.
- ASTM F1797-98 (2003) Standard test method for acoustic emission testing of insulated digger derricks.
- amplitude and frequency analysis
- source location
- fracto-emission
- vibration and damping [25, 26]
Leavey et al [27] have presented an introductory
tutorial on the use of wavelet analysis for signal processing in this context. Yella et al [28] have recently reviewed the use of artificial intelligence
techniques for the automatic interpretation of data from NDT. Addin et al [29] have reviewed the use of neural networks in the prediction and
detection of failures in laminated composite materials, with specific reference to NDT by vibration mode and frequency, use of Lamb waves and electrical
conductivity. Gros [30, 31]
has reviewed the use of data fusion for handling multiple data sources in NDT.
Backman [32, 33] has considered how safety methods can be made available to the
engineering community without requiring huge statistical databases for use in
reliability analysis. The book considers the probability of safe flight,
and is thus perhaps essential reading for those involved in aerospace structural
design, although much of the analysis is undertaken at the level of orders of
magnitude rather than in fine detail. Of particular relevance here is the
consideration of probability of detection against damage size for various
regions [Figure 1] and the ability of each non-destructive testing technique
relative to the respective damage sizes. Wall et al [34] have considered
probability of detection (POD) data in industrial applications and suggest that
could be benefits from the use of simple POD generator models validated against
experimental data with a more structured and standardised approach to the use
and correction of POD data (using expert judgement, modelling and signal-based
methods).

Figure 1: Probability of Detection (POD) against damage size (after Backman
[32]).The various NDT techniques have an
important role to play in both
Condition Monitoring (CM) and
Structural Health Monitoring (SHM) which are covered in a lecture delivered
to both module
MECH512 Design for Structural Integrity and
MECH 513 Smart Materials and
Intelligent Structural Systems.
Resources:
- HIGHLY RECOMMENDED: Seeing is believing: basic ultrasonics,
Services Sound and Vision Corporation (Ministry of Defence), 1987.
UOP Library.
This VHS videocassette recording used Schlieren photography
to visualise ultrasound pulses travelling in a glass block.
References:
- John Summerscales, Non-destructive testing of advanced composites: a review of recent advances,
British Journal of Non-Destructive Testing, November 1990, 32(11) pp 568-577.
Restricted:
Download 2.25MB .doc file.
This version has additional images.
- J Summerscales, Non-destructive measurement of the moisture content in fibre reinforced plastics,
British Journal of Non-Destructive Testing, February 1994, 36(2), pp 64-72. Restricted:
Download 1.21 MB .pdf file
- J Summerscales, Manufacturing Defects in Fibre Reinforced Plastics Composites,
Insight, December 1994, 36(12), pp 936-942.Restricted:
Download 1.04 MB .pdf file.
This paper considers the appropriate NDT techniques.
- EA Birt and RA Smith,
A review of NDE methods for porosity measurement in
fibre-reinforced polymer composites
This paper - which first appeared in Insight - Non-Destructive Testing and
Condition Monitoring
(The Journal of the British Institute of Non-Destructive Testing), November
2004, Vol. 46, No. 11, pp 681-686.
- is made available here to University of Plymouth students
Restricted:
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with the kind permission of the British Institute of Non-Destructive Testing,
the authors and QinetiQ Ltd.
The authors are with the NDE Group, QinetiQ, A7 Building,
Cody Technology Park, Farnborough, Hampshire GU14 0LX.
E-mail: eabirt~@~QinetiQ.com (remove the tildes from the quoted e-mail before
use).
- SR Stock,
X-ray microtomography of materials, International Materials Reviews, April
1999, 44(4), 141-164.
- F Desplentere, SV Lomov, DL Woerderman, I Verpoest, M Wevers and A
Bogdanovich,
Micro-CT characterization of variability in 3D textile architecture,
Composites Science and Technology, October 2005, 65(13), 1920-1930.
- PJ Schilling, BPR Karedla, AK Tatiparthi, MA Verges and PD Herrington,
X-ray computed
microtomography of internal damage in fiber reinforced polymer matrix
composites, Composites Science and Technology, November 2005, 65(14),
2071-2078.
- H Shang and J Gao, Theories and industrial applications of optical interferometric NDT techniques: a review, Insight, May 2009, 51(5), 240-251.
- A Mujeeb, VU Nayar and VR Ravindran,
Electronic Speckle Pattern Interferometry techniques for non-destructive evaluation: a review,
Insight, May 2006, 48(5), 275-281.
- P Pallav, G Diamond, D Hutchins and TH Gan, A near infrared technique for
non-destructive evaluation, Insight, May 2008, 50(5), 244-248.
- Infrared Thermography Handbooks (British Institute of Non-Destructive
Testing Condition Monitoring Series):
Norman Walker, Volume 1 - Principles and Practice. ISBN 0-903132-33-8. AN
Nowicki, Volume 2 - Applications. ISBN 0-903132-32-x.
- KK Ghosh and VM Karbhari,
A critical review of infrared thermography as a method for non-destructive evaluation of FRP rehabilitated structures, International Journal of Materials and Product Technology, 2006, 25(4), 241-266.
- PH Siegel, Terahertz technology, IEEE Transactions on Microwave Theory and Techniques, March 2002, 50(3), 910-928.
- DL Woolard, ER Brown, M Pepper and M Kemp, Terahertz frequency sensing and imaging: a time of reckoning future applications?, Proceedings of the IEEE, October 2005, 93(10), 1722-1743.
- Roger Appleby and H Bruce Wallace, Standoff detection of weapons and contraband in the 100 GHz to 1 THz Region, IEEE Transactions on Antennas and Propagation, November 2007, 55(11/1), 2944-2956.
- AG Davies, AD Burnett, W Fan, EH Linfield and JE Cunningham,
Terahertz spectroscopy of explosives and drugs, Materials Today, March 2008, 11(3), 18-26.
- N Yu, QJ Wang, MA Kats, JA Fan, SP Khanna, L Li, AG Davies, EH Linfield and F Capasso, Designer
spoof surface plasmon structures collimate terahertz laser beams, Nature: Materials, September 2010, 9(.), 730-735.
- RA Pethrick and D Hayward,
Real time dielectric relaxation studies of
dynamic polymeric systems, Progress in Polymer Science, 2002, 27(9), 1983-2017.
- Koji Asami, Characterization of heterogeneous systems by dielectric
spectroscopy, Progress in Polymer Science, 2002, 27(8), 1617-1659.
- Gi Xue, Fourier transform Raman spectroscopy and its application for the
analysis of polymeric materials, Progress in Polymer Science, 1997, 22(2)
313-406.
- G Kotsikos, AG Gibson and J Mawella,
Assessment of moisture
absorption in marine GRP laminates with aid of nuclear magnetic resonance
imaging, Plastics, Rubber and Composites, 2007, 36(9), 413-418.
- BW Drinkwater and PD Wilcox,
Ultrasonic arrays for non-destructive
evaluation: a review, NDT & E International, 2006, 39(7), 525-541.
- M Moles, N Dubé, S Labbé and E Ginzel,
Review of ultrasonic phased arrays for pressure vessel and pipeline weld
inspections, Journal of Pressure Vessel Technology, August 2005, 127(3),
351-356.
- RA Smith, LJ Nelson, MJ Mienczakowski and RE Challis,
Automated analysis and advanced defect characterisation from ultrasonic scans of composites, Insight, February 2009, 51(2), 82-87.
- R Chandra, SP Singh and K Gupta,
Damping studies in fibre-reinforced composites, Composite Structures, 1999,
46(1), 41-51.
- Y Zou, L Tong and GP Steven,
Vibration-based
model-dependent damage (delamination) identification and health monitoring
for composite structures - a review, Journal of Sound and Vibration,
2000, 230(2), 357-378.
- CM Leavey, MN James, J Summerscales and R Sutton,
An introduction to wavelet transforms: a tutorial approach, Insight, May 2003, 45(5), 344-353.
Restricted:
Download 1.04MB .pdf file.
This paper describes recent developments in
signal processing.
- S Yella, MS Dougherty and NK Gupta,
Artificial intelligence techniques for
the automatic interpretation of data from non-destructive testing,
Insight, January 2006, 48(1), 10-20.
- AO Addin, SM Sapuan, E Mahdi and M Othman,
Prediction and detection of failures in laminated composite materials using
neural networks - a review, Polymers and Polymer Composites, 2006,
14(4), 433-441.
- XE Gros, NDT Data Fusion, Butterworth-Heinemann, 1997. ISBN:
0-340-67648-5.
UOP Library
- XE Gros, Applications of NDT Data Fusion, Kluwer Academic Publishers,
Dordrecht (NL), 2001. ISBN: 0-7923-7412-6.
- Bjorn Backman,
Composite Structures, Design, Safety and Innovation,
Elsevier, Amsterdam, 2005. ISBN 0-08-044545-4.
UOP Library
- Bjorn Backman,
Composite Structures: Safety Management,
Elsevier Science, May 2008. ISBN-13: 978-0-08-054809-8.
- M Wall, SF Burch and J Lilley, Review of models and simulators for NDT reliability (POD), Insight, November 2009, 51(11), 612-619.
TeraHertz spectroscopy for NDT of composites
- K Naito, Y Kagawa, S Utsuno, T Naganuma and K Kurihara,
Dielectric properties of eight-harness-stain fabric glass fiber reinforced polyimide matrix composite in the THz frequency range, NDT & E International,
July 2009, 42(5), 441-445.
- K Naito, Y Kagawa, S Utsuno, T Naganuma and K Kurihara,
Dielectric properties of woven fabric glass fiber reinforced polymer-matrix composites in the THz frequency range, Composites Science and Technology, September 2009, 69(11-12), 2027-2029.
- C Jördens, M Scheller, S Wietzke, D Romeike, C Jansen, T Zentgraf, K Wiesauer, V Reisecker and M Koch,
Terahertz spectroscopy to study the orientation of glass fibres in reinforced plastics,
Composites Science and Technology, March 2010, 70(3), 472-477.
- C Stoik, M Bohn and J Blackshire,
Nondestructive evaluation of aircraft composites using reflective terahertz time domain spectroscopy, NDT & E International, March 2010, 43(2), 106-115.
Further reading
- David J Smith,
Reliability, Maintainability and Risk - Practical Methods for Engineers
including Reliability Centred Maintenance and Safety-Related Systems -
seventh edition, Elsevier, 2005. ISBN13: 9780-7506-6694-7.
UOP Library
- J Summerscales,
Non-Destructive Testing of Fibre Reinforced Plastics Composites - volume 1,
Elsevier Applied Science Publishers, Barking UK, September 1987.
ISBN 1-85166-093-3. Now distributed by Springer.
UOP Library
-
J Summerscales,
Non-Destructive Testing of Fibre Reinforced Plastics Composites - volume 2,
Elsevier Applied Science Publishers, Barking, 1990.
ISBN 1-85166-468-8. Now distributed by Springer.
UOP Library
-
BW Drinkwater and PD Wilcox -
Ultrasonic arrays for non-destructive evaluation:
A review, NDT & E International, 2006, 39(7), 525-541.
-
RA Pethrick and D Hayward -
Real time dielectric relaxation studies of dynamic
polymeric systems, Progress in Polymer Science, 2002, 27(9), 1983-2017.
-
Koji Asami - Characterization of heterogeneous systems by dielectric
spectroscopy, Progress in Polymer Science, 2002, 27(8), 1617-1659.
Elsevier ScienceDirect
- R Chandra, SP Singh and K Gupta -
Damping studies in fiber-reinforced
composites: a review, Composite Structures, 1999, 46(1), 41-51.
-
Gi Xue [231 references],
Fourier transform
Raman spectroscopy and its application for the analysis of polymeric materials,
Progress in Polymer Science, 1997, 22(2) 313-406.
-
MA Drewry and GA Georgiou [10 references], A review of NDT techniques for wind
turbines, Insight, March 2007, 49(3), 137-141.
The British Institute of Non-Destructive Testing has published a useful series
of introductory texts under the title NDT
Fundamentals,
The ultrasonics papers are made available here to University of Plymouth students
with the kind permission of the British Institute of Non-Destructive Testing and
of the author.
- JC Drury, Ultrasonics, part 1: basic principles of sound, Insight, November 2004, 46(11), 650-652.
Restricted:
Download 199KB .pdf file
- JC Drury, Ultrasonics, part 2: properties of sound waves, Insight, December 2004, 46(12), 762-764.
Restricted:
Download 324KB .pdf file
- JC Drury, Ultrasonics, part 3: refraction and mode conversion, Insight, January 2005, 47(1), 44-46.
Restricted:
Download 209KB .pdf file
- JC Drury, Ultrasonics, part 4: transducers for generating and detecting sound waves, Insight, February 2005, 47(2), 98-100.
Restricted:
Download 265KB .pdf file
- JC Drury, Ultrasonics, part 5: probe construction, Insight, March 2005, 47(3), 168-171.
Restricted:
Download 594KB .pdf file
- JC Drury, Ultrasonics, part 6: pulse-echo flaw detector, Insight, April 2005, 47(4), 236-238.
Restricted:
Download 350KB .pdf file
- JC Drury, Ultrasonics, part 7: the ultrasonic beam, Insight, May 2005, 47(5), 297-299.
Restricted:
Download 239KB .pdf file
- JC Drury, Ultrasonics, part 8: calibration and reference standards, Insight, June 2005, 47(6), 364-365.
Restricted:
Download 159KB .pdf file
- JC Drury, Ultrasonics, part 9: compression wave techniques, Insight, July 2005, 47(7), 425-428.
Restricted:
Download 464KB pdf file
- JC Drury, Ultrasonics, part 10: shear wave techniques, Insight, August 2005, 47(8), 495-499.
Restricted:
Download 301KB pdf file
- JC Drury, Ultrasonics, part 11: surface and TOFD techniques, Insight,
September 2005, 47(9), 569-571. Restricted:
Download 428 KB pdf file
- S Cochran, Ultrasonics, part 12: fundamentals of ultrasonic phased arrays,
Insight, April 2006, 48(4), 212-217. Restricted:
Download 756 KB pdf file
- J Hansen, The Eddy current inspection method, part 1: history and
electrical theory, Insight, May 2004, 46(5), 279-281.
- J Hansen, The Eddy current inspection method, part 2: the impedance plane
and probes, Insight, June 2004, 46(6), 364-365.
- J Hansen, The Eddy current inspection method, part 3: instrumentation and
applications, Insight, July 2004, 46(7), 414-416.
-
J Hansen, The Eddy current inspection method, part 4: applications,
practical testing and advanced concepts, Insight, August 2004, 46(8), 480-483.
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Updated by John Summerscales on
10 October 2011 13:10. Terms and conditions. Errors and omissions. Corrections.